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5 EXTRACTION METHODS

5.1 SOLVENT EXTRACTION


Use: Analyte extraction from soil and ground water samples. Simplified extraction procedures have been developed for field screening of PCBs, PAHs, and pesticides.

Description:

Solvent extraction procedures involve the use of one more organic solvents, acids, or other chemical substances and measures, such as filtration and centrifugation, to remove and concentrate the analyte of interest.

Analytes:

1. Non-Halogenated VOCs 5. PAHs 9. Inorganics
2. Non-Halogenated SVOCs 6. Pesticides/Herbicides 10. Explosives
3. Halogenated VOCs 7. Metals 11. TPHs
4. Halogenated SVOCs 8. Radionuclides

Media:

Soil: Ground Water: Surface Water: Gas/Air:
MINIMUM MODERATE MODERATE Not Applicable
Maximum Depth: Not Applicable.
Production Rate: Sample is available after a short amount of time.
Investigation Derived Waste Volume: Large volume of waste.
Technology Status: Commercially available technology with moderate field experience.
Certification/Verification: Technology has not participated in CalEPA certification and/or CSCT verification program.
Relative Cost per Sample: Mid-range expense.

Limitations:

ASTM Standards:

D 5765 - 95 Practice for Solvent Extraction of Total Petroleum Hydrocarbons from Soils and Sediments Using Closed Vessel Microwave Heating.

EPA Methods:

3500B Organic Extraction and Sample Preparation.
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